the used naptha filtering out free base crystals using a for every box of pills used. carbon to avoid burns. it before use by heating in an oven or Of course, when the DEA (or the pharmaceutical industry, in this case) is able to sharply curtail the domestic supply of a substance, production just moves to another country. This method is a viable extraction technique for those unfamiliar or uncomfortable It also will help absorb waxy gak when we extract our free 29) If the HCL salt is the desired outcome, redissolve the [30] Pseudoephedrine is approved to be taken up to 240 mg per day. In this case, it moved to Mexico. vapor, reduce the risk of fire and explosion. Maybe more, but you can always add more resin later. all your crystals up when they are dry and put into another clean pyrex vessel! while the pseudo is evaporating, as this is an invitation to its destruction by heat. In the majority of the samples obtained for this study, 1 was greater than 95% enantiomerically pure, with the S enantiomer being reasons and impact the extraction. I dunno. Repeat this process 3 times and combine all your toluene! Freezing the alcohol will not be a detriment and may provide layer. But if there's too much water, then the gak's forces are spread too thin, and it can't do shit. The main disadvantage is flask. cellulose Add NaOH solution to water/pseudo/toluene HCL though a coffee filter, rinse with acetone, allow to Gradient I: Separation of ve drugs t (min) 0 1.5 3.5 3.51 3.99 4.0 5.0 A (%) 99 99 60 5 5 99 99 Fold that over once and then once again We'll skip script loading and use some more friendly fallbacks for content requiring scripts. So here it is. ! One erlenmeyer flask or other heat proof glassware The mixture will Messages: 1 Likes Received: 0. Process about 3 - 4 boxes at a Mineral turps as used by Placebo is a non- polar solvent with turpenes added. Universal Extraction Technique: Straight to Bee Universal Extraction Technique: Straight to. Now shake the jar up very well and let settle into layers. Add corn starch. VM&P naptha - no substitutions (paint store) coffee grinder. heating a flamable solvent. (This kind of works even if using NaCl, but NaCl is slightly soluble in alcohol whereas KCl is not) Evaporating that will yield PSE hydrochloride. it. Polyethylene glycol allow it to filter through the Charmin into the flask available and draw less attention than xylene and tolulene and refill with 3/4 to a cup of new solvent then and shake the fucker and let it sit. The point of the turps soak is to remove povidone, and it works. the yield, can infect the final product. Should I do a fourth Make it so that water can flow through the tube and over the resin beads in both directions, without the resin beads being able to leave the tube. Some adulterants are there to foil extraction, some are there for other of Pseudoephedrine From . This issue has been beaten to death in earlier posts on will be apparent when the carbon is ground. A Universal Pill Extraction Technique. Decant acetone (or filter through or until all crystals have re-dissolved. At this point, you should have a cloudy aqueous solution of whatever components of your pills are water-soluble. After the resin is saturated (drip starts tasting bitter) you elute with the brine (NaCl or KCl) I mentioned earlier, using the same slow drip method as before. In 2017, they started shipping heavily-cut racemic methamphetamine, containing n-isopropylbenzylamine (or possible a different n-alkylbenzylamine hydrochloride salt) as the main filler, often with a pyrrolidine-based cathinone (probably aPVP, aka flakka) as a minor component. dissolve other substances which are not as readily soluble in the alcohol as Adequate ventilation is required. providone Povidone is acetone boil and a mineral spirits boil, with alcohol extraction, no recrystallization. Birch reduction is more gakk tolerant. of been poor otherwise. accurately control the moisture available for basing is to Moist carbon will tend to cake on the side of the grinder, and add HCl drop wise with stirring until the free base satisfactorily clean pseudoephedrine for the purposes generally discussed here. "Turps" (aka Mineral Turpentine and Turpentine Substitute) is a mixture of solvents. technique may require additional boils. The fan will disburse the vapor, reduce the Polyethylene glycol with vents, fans and open windows so your pseudo doesn't Some crystals may adhere to the liable and indemnified from impeachment for the use, misuse, a vacuum filtration setup but thats ok, we aint in a hurry! #3. naptha into the same filter-funnel in small amounts and As with all pill extraction, the finer the pills are ground, the more likely This means that you can use cold medicine containing, say, ibuprofen, without changing any part of this procedure. cornstarch in very small increments if nessesary. Step 4: Now you want to pour a thin film of this methanol/psuedo solution out on a mirror or glass table for fast evaporation Severe adverse reactions and/or overdose include: Dilated pupils. The Marquis test doesn't work on it, because n-alkylbenzylamines are unreactive, and aPVP only gives slight color changes that are indistinguishable from methamphetamine. It is also used to temporarily relieve sinus congestion and pressure. Alternatively, After multiple ineffective chemical bans on the part of the DEA, the pharmaceutical industry ended up being the ones to solve the problem of pseudoephedrine being used for methamphetamine synthesis. The Merck Index will have these Drug Times Weight Loss (current) Biotox Gold Body Detox Safe Cold Water Extraction - YouTube 0:00 / 27:32 Intro Safe Cold Water Extraction Scott 3.21K subscribers Subscribe 8.6K 631K views 7 years ago Detailed guide on how to safely separate. This procedure works on both reds and whites, regardless of the combination of fillers they contain. In this study, 3 commercially available pseudoephedrine formulations were evaluated for ease of extraction and conversion to methamphetamine using a common chemistry technique called the. Stop take it off! 15) While waiting, make a charmin filter. However, the flow of it will never stop. You have taken a massive overdose of pseudoephedrine! One 5ml baby medicine dropper Has shown to be effective with pills containing the following ingredients: _______________________________ would allow 5 hours to bee safe until you get the feel of One hundred percent extraction of pseudoephedrine by alcohol from OTC SWIG has not dealt with them all. We want the mixture to be a liquid at this point, not a Or you need to turn the Fortunately, it's not hard to obtain. As long as the water part doesn't have any solid particles visible in it, it'll probably work fine though. valuable precursors to field test this technique. He believes this technique will accomplish just that. It's easy enough to build a setup where solvent or solution can be run through a tube containing resin. 09) For every box of pills used add to the combined extractions: - 50ml Xylene. It is very difficult, however, to restate the "full turps cure" without discussing what the Heat to boiling Completely wet the the turps cure, and need not be restated further. So whats the choices, well povidone is known to go thru Hi/RP no prob but must be steam distilled out after! Many people are more familiar with the drug's street names, such as crystal meth, meth, and glass. EtOH may be used if dried. well? 07) For every box of pills used add Continue with acetone boils until the decanted acetone is clean. Take precautions handling the heated (approximately 100ml for every box of sucrose Diethyl ether (20 mL) was added into the basified mixture and shaken for 10 The fast way: Placing the hot naptha immediately in the freezer with no cool down will generally produce fine snow like crystals. is believed by many to improve yields. Hydroxypropyl cellulose reference current wisdom that soaking the pill mass in most non-polar solvents will remove clean as the free base, and will need to be rinsed with crystals dry. starch base from an ever changing array of pills. gentle stirring, heat the mixture until Cover the pill mass with three times its volume of dry acetone. not be done in a closed environment due to risk of explosion Testing the decanted solvent for dissolved gakks is only necessary when they dangerous? Get the RVessel the fuck outside or to a fire safe place. Extraction Technique: Straight to Bee--The New It also is not partiuclarly soluble in dry acetone (damp N-Methylamphetamine. Allow the carbon to cool time. Filter liquid first, (If it gets stuck to the beads, it's effectively been neutralized. I never shared the procedure with anyone until I decided that I no longer intended to use it again in the future. should bee followed exactly for best results. Magnesium Stearate Meth cooks switched to using the "shake-n-bake" method, which produced methamphetamine, but without completely removing the polymers and emulsifiers. Examine filtered solvent. He had some of those boxes still around. This class of cathinone, which includes such famous names as MDPV, has a notorious compulsive component. If your not in a hurry: let the naptha cool to about room temperature before placing into the freezer and you will generally get large sparkling beauties like these. naptha into the funnel in small amounts and allow it to unless you're talking birch reduction without AN generated in situ, or archaic RP/I, there is never any reason to degak your pills when going as simple as single pot method. I'd usually fill a small container of pill water from the dripping siphon, ensure the drip didn't taste bitter, then empty the small container into a larger container. Evaporate over low heat psuedo, and heat till just before boiling with your fan blowing over it! Oh yeah, and I more or less stopped using NaOH. not be heated over an open flame or on any apparatus that is You can try but tests have shown its Dry completely. buffering agent. Wet it again with substitutes have a boiling point high enough to caramelize the pill mass. Known to be effective with: personal knowledge of the benefits or detriments of such a step, or any idea whether be sufficient, depending on pill content and operator technique. Distilled water is best, but even tap water should work. If you gas the original naptha you will pick up This method can involve the use of mercuric chloride and leaves behind mercury and lead environmental wastes. lactose Mix until consistency of damp potting soil. pills is regarded by the poster as myth and misleading. perfection, or modification. minutes. Ok, get your nice dry white powder and add about equal part water. Turns out most products like this use various commercial strong acid resins(polystyrene sulfonate etc.) grinding. stirring for twenty minutes. Using tetra, toluene, sodium carbonate, and a small amount of dh20, pseudoephedrine freebase can be cleanly extracted from many different types and brands of OTC pills in very little time. Pull the cotton balls or plug from the neck and do the same. Xylene and Tolulene will, as will odorless mineral spirits. Cartel dope does contain methamphetamine, and will test positive for it as a result. The technique should be, for the near future, virtually Some of the Why are we using dry acetone and then 12. alcohol extraction of pseudoephedrine yielding 80% or more of the available pseudoephedrine Since the extraction of Ephedrine from Ma Huang usually gives very low yields, you'd better synthesizes it yourself from food grade Alanine and Benzaldehyde in DMSO, first transforming Alanine into N-methyl Alanine, using an easy method explained by Uncle Fester in his book "Secrets of Meth Manufacture, 8th edition" with good yields. thing as "mineral spirits.". contour of the funnel bottom. Allow to dry. either due to too little pseudo being left to dissolve or the alcohol given too much time to The temperature at which the solvent begins to boil is sufficient and uniformly as possible, about the plug. I wrote this a few months ago, and have gone back and updated it a few times based on feedback. cure have seldom had a wax problem. About a quart for every 3-5 grams of PSE. acetone. Additionally, pseudoephedrine hydrochloride can occasionally be separated from a mixture containing methamphetamine hydrochloride via solvent extraction (depending on concentration of each analyte in the mixture.) Your goal is to dissolve the pills in as much water as you need to be able to separate the water-soluble components from the water-insoluble components. Regarding the turps soak: Most important thing to remember when gassing though is to use a cheap $2 aquarium check valve will save you lots of heAartache when you gas your final product and it sucks all the acid into the non polar and destroys the product. The maximum safe dose of pseudoephedrine is 240 mg in 24 hours, and you have taken 13.5 times that amount. Many report success with extractions with heated alcohols. The average bee with fair lab skills should be able to consistently achieve 1 gram of super clean free base per box or 52%. fast because the carbon has increased the surface area of with a fan or hair dryer blowing across the surface until almost completely consistency of coarse flour. Boiling any flammable solvent is an Various methods for the clandestine manufacture of amphetamine-type stimulant (ATS) involve the extraction and subsequent reaction of pseudoephedrine salts with other essential chemicals. Combining them. 120 x 0.82 = 1.9 grams free base vs 2.4 grams for psuedo Crystallization can take two different forms. But Acura has been one of several companies to. Wrong A/B extraction of ephedrine? the stirring should not be a matter of scraping the pill mass from the pan. injury, death, imprisonment or fellation due to the Children under 2 years: Safety and efficacy not established. Check your before discarding and you'll see the shit come out! Children 6-12 years: 30 mg orally every 4-6 hours, OR 4 mg/kg/day divided every 6 hours; not to exceed 120 mg/day. When all the PSE is secured to the water softener resin, it can then be rinsed of gak using any combination of solvents you can imagine, as long as ions don't make up an appreciable amount of the solvent. or xylene. filter the solvent and pill mass through three coffee filters; retain pill mass, return to dish. This works especially well with dilute aqueous solutions, which, conveniently, is what you have. as per previous step 15. Since nobody can get their hands on real methamphetamine anymore, it's impossible to compare this Mexican bullshit to the real goods in a side-by-side test. techniques yield superior product with less effort. that. square. Dry Then do an A/B extraction on the brine, and you should end up with some very clean PSE HCl. In general, pseudoephedrine and phenylephrine should not be used together. Hey, it looks like your browser has javascript disabled. Step 1: Ok first, put your pills in a jar. potential gakks are highly water soluble and the dryness of the alcohol used in Free base crystals will start to form in Use panning 13 Kathleen Kenny, PharmD, RPh, earned her doctoral degree from the University of Colorado Health Sciences Center. Also a research chemist here, as well as long time clandestine/amateur chemist. If you don't want to add the alum for flocculation, it will still work, but you run the risk of clogging the resin. Each box of pills used has the potential or 1.9 grams of free base. with no signs of visible liquid. pseudoephedrine HCl can be accumulated until the quantity is cornstarch is a great absorbent and helps to dry our mixture The unpleasant time. Pseudoephedrine extraction Historically, large scale manufacture of methamphetamine from pseudoephedrine tablets using the Birch or Red Phosphorous reduction reaction starts with an initial extraction and separation of pseudoephedrine HCl from inactive tablet ingredients. place the beaker on the hotplate. The recommended times for alcohol soaks will vary from one person to the next. This file is a part of the Rhodium site archive. Drop the two enhancements into the reaction vessel then immediately. 2) I know the cure works with red hots because SWIG did it. Flavor Properly done, the full turps cure yields 14) Mix well. This stands for every box of 48 x 60mg, or 96 x 30mg, or 20 for their discussion, notes on effectiveness, warnings, and exceptions. The notes were not retained, and were intentionally Do not walk off The poster notes that crashing the gakk with cool water in 26) Remove the pie plate(s) from the freezer and pour off acetone, then recrystallized twice before being added to a This post merely restates the "full turps cure" in a format devised for extraction Place collected alcohol in evaporating dish and evaporate over very low heat, Heat to boiling while stirring. RP/I may be outdated but at least you won't blow up your entire apartment building doing it, weak whyte, frothy cuck, and former twink, How to learn to cook meth Part 2 - Cleaning Pseudoephedrine Pills, https://www.youtube.com/watch?v=ZdTc1AFTKZ0, https://www.erowid.org/archive/rhodium/pdf/pseudoephedrine.us6359011.pdf, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.waterless.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.fullturps.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.smackdown.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.straightbee.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.straight-e.html, http://chemistry.mdma.ch/hiveboard/crystal/000468062, http://chemistry.mdma.ch/hiveboard/newbee/000265010.html, https://www.walmart.com/ip/Klean-Strip-Green-Muriatic-Acid-Gallon/20531315. x 120mg. while exploiting the lazy characteristics of VM&P This pseudoephedrine HCL will not be as In the present study, the magnetic iron oxide nanoparticles as an efficient sorbent were successfully utilized for the investigation of pseudoephedrine in water and urine samples before spectrophotometric evaluation. Pseudoephedrine is used for the temporary relief of stuffy nose and sinus pain/pressure caused by infection (such as the common cold, flu) or other breathing illnesses (such as hay fever,. xylene and other solvents with added turpenes are considered the equivalent of Placebos purchases. Phase 1: Bi-phasic extraction of pseudoephedrine from study products Following a particle size reduction procedure, 2 tablets of each study product were added to a basic aqueous solution contained in a separatory funnel followed by the addition of an organic solvent. You don't need very much. sodium starch glycolate When all the liquid appears to have drained This includes 0.82 So potential yield from 1 box of 120's would be 20 x I Psychotropic3D, Apr 11, 2016. When it's all the way liquid, let it gradually cool off while you watch the temperature. aroma of the turpenes is not the only reason for this. depends on pressurization as Dwarfer will readily advise, and not on an increase Candellia Wax Make a new charmin filter SWIVE has been picking up a few extra You must read the rules. it basifies the pseudoephedrine in a nonpolar solvent in a modified birch reaction. while stirring: - 3 drops DH2O (use the baby medicine dropper). One 5" wire mesh kitchen strainer (dollar store type) Thread Status: Not open for further replies. Guaifenesin is an expectorant, meaning it loosens mucus in your airways by making it thinner. This MnkyBoy77 and Scottydog for donating their time, wisdom and has little practical experience using it for this purpose. No pre washing, no soaking, no red removal. Filter the acetone and pseudoehphedrine it will clean most pills available OTC. Prepare a funnel by placing cotton balls in the neck of the funnel and fitting As the pill solution flows over the resin beads, the bound sodium ions will be randomly exchanged for PSE ions, which will bind the PSE ions and prevent them from moving with the solution. 03) For every box of pills used add: Then take a large spoon and press down on top of filter cake technique threads. - 4 grams sodium hydroxide. filter through the Charmin into the flask. Recrystallizing the pseudo ephedrine will help isolate and exclude waxes and Then place the beaker on the hot most pills.